NAME Structural Integrity Unit

DESCRIPTION

The unit combines a complete testing equipment for the mechanical characterization of materials and components and the expertise to extract meaningful information from the tests. Testing includes dynamic loadings from very small strain rates (1 µm/hour, typical of creep at elevated temperatures), up to 14 m/s (impact tests). Testing frequencies range from 1 cycle in several minutes (thermo-mechanical fatigue tests) to 200 Hz (in resonant fatigue testing machines). Loading can be uniaxial (tension-compression) or biaxial (tension-compression plus torsion), within a temperature ranging from liquid nitrogen (77 K) up to 1200 °C. Strains are measured (measuring hysteresis loops) at all temperatures and environments. Fatigue limit and complete S-N (stress vs. number of cycles or time) curves can be determined for real materials, components and structures. Artificial micro-defects can be introduced by Focused Ion Beam (FIB) milling, when required on testing samples. Interfaces between different materials (surface depositions, coatings) can be characterized determining bonding energy and interface toughness. Early crack detection is available through Infrared Thermography with a resolution of 10 µm. Residual and total life assessment are deduced, including effects of local residual stresses. Residual stresses are obtained by x-ray diffraction. Local residual stresses are measured -by FIB and Digital Image Correlation (DIC)- at the microscale level.

FIELDS OF APPLICATION

Advanced unions

Coatings and Surfaces solutions

Design and development of materials

Manufacturing processes

MOST OUTSTANDING EQUIPMENT AND COMPONENTS

  • Electromechanical fatigue testing machine (1 µm/h), Instron 8562

    Electromechanical fatigue testing machine (1 µm/h), Instron 8562

  • Focused Ion Beam (FIB) milling. Quanta 3D FEG

    Focused Ion Beam (FIB) milling. Quanta 3D FEG

  • Nano-indenter & TriboIndenter

    Nano-indenter & TriboIndenter

  • Servo-hydraulic fatigue testing machine, Instron, ± 250 kN

    Servo-hydraulic fatigue testing machine, Instron, ± 250 kN

  • Servo-hydraulic tension-torsion fatigue testing machine, Instron 8874

    Servo-hydraulic tension-torsion fatigue testing machine, Instron 8874

SERVICES OFFERED BY THE ASSET

Characterization of Interfaces

Mechanical and structural characterization of surfaces and coatings (Atomic Force Microscopy (AFM), nano-indentation, residual stresses, FIB milling, X-ray diffraction). Bonding energy, interface toughness, weakest fracture path.

Forensic failure analysis

Analysis of in-service components and forensic analysis of failures.

Life assessment

Life assessment of components including the effect of stress fields, complex thermal cycles (TMF) and residual stresses.

Measurement of mechanical properties

Measurement of mechanical properties and their scatter (fatigue limit, S-N curves, toughness) under in-service conditions (stresses, temperatures, environment, cycles…), minimizing safety coefficients and production costs.

ENTITY MANAGING THE ASSET

ENTITY MANAGING THE ASSET
CEIT
Contact person:
Asier Bergara Arregui
abergara@ceit.es